Ministry of Education and Science of the Republic of Kazakhstan
Karaganda State Technical University
Confirmed by
Chairman of the Academic Council,
rector, RK NAS academician
Gazaliyev A.M.
_______________________
_________ ____, 20___.
Syllabus
Course PCRE 4308 “Protective coatings and refractory enamels”
MPR 34 “Protective coatings and refractory enamels”
Major5В071000 – Materials Science and Technology of New Materials
Mechanical engineering Institute
Department of Metallurgy, Materials Science and Nanotechnology
2013
Preface
Syllabus is worked out by cand.of Sc., Professor Sharaya O.A, Senior tutor Yudakova V.A.
Discussed at the meeting of the department «Metallurgy, Materials Science and Nanotechnologies»
Minutes № _______ of ______________ «____» 20___
Head of department ________________ ___________«____» 20___
(signature)
Approved by the Educational Council of the Mechanical Engineering Institute
Minutes № _______ of ______________ «____» 20___
Chairman ________________ ____________ «____» 20___
(signature)
Tutor’s personal data and contact information
Cand.of Sc., Professor Sharaya O.A, Senior tutor Yudakova V.A.
«Metallurgy, Materials Science and Nanotechnology» chair is in the main building of KSTU, B. Mira, 56 room No.313, contact phone 56-59-35 add. 1024 .
Course labour intensity
Term
|
Number of credits / ЕCTS |
The type of classes |
number of AL |
Total number of hours |
Forms of Control |
||||
number of contact hours |
number of Office hours |
Total hours |
|||||||
lectures |
practical classes |
laboratory classes |
|||||||
8 |
3/5 |
30 |
15 |
– |
45 |
90 |
45 |
135 |
Examination |
Course description
Course «Protective coatings and refractory enamel» is profile subject required for training-materials science specialists. Knowledge of basic methods for applying protective and decorative coatings for graduates to understand the formation and the ability to develop high-technology coating process.
Course purpose
The purpose of this course is to study the general aspects of the theory and practice of the application of all types of protective and decorative coatings.
Course objectives
As a result of studying of this course:
student knows:
– Classification of all methods of coating, both internal and external;
– The methods of evaluation of quality indicators;
– The physico-chemical properties of solid surfaces;
– The physico-chemical properties of materials for coating;
– basic common parameters and patterns:
– Gas thermal spray coating;
– Vacuum condensation coating;
– Coating of a molten state;
student is able:
– To analyze the structural features of products and the conditions of their service;
– To develop optimal mode settings coating process;
– Choose the method of coating.
Prerequisites
Studying of this course requires assimilation of the following courses (with the indication of sections (subjects)):
Course | Titles of sections (subjects) |
1. Physics | Structure and properties of metals |
2. Chemistry | Thermodynamics |
Kinetics | |
3. Physical and Colloid Chemistry | Laws of valence |
The nature of the chemical bonds | |
Diffusion Processes | |
Chemical Thermodynamics | |
Kinetics | |
4. Engineering materials. | Full course. |
5. The physical properties of materials. | Full course. |
6. The mechanical properties of materials. | Full course. |
Postrequisites
The knowledge received at studying of course «Protective coatings and refractory enamel» is used at implementation of special sections of the degree project (work).
1. Physical materials.
2. Modern methods of materials research.
Thematic plan of the course
Name of section (subject) |
Complexity by types of classes, hours. |
||||
Lectures |
practical |
laboratory |
OH |
AL |
|
Theme 1. Introduction. The classification covers. Internal and external coating. |
2 |
4 |
|
5 |
5 |
Theme 2. Selection process of coating |
2 |
|
|
4 |
4 |
Theme 3. Physico-chemical properties of the solid surface. |
2 |
|
|
4 |
4 |
Theme 4. Physical and chemical properties of the coating. |
2 |
3 |
|
4 |
4 |
Theme 5. Thermal spray coating. |
2 |
4 |
|
5 |
5 |
Theme 6. Vacuum condensation coating. |
2 |
4 |
|
4 |
4 |
Theme 7. Coating from the molten state. |
3 |
|
|
4 |
4 |
TOTAL: |
15 |
15 |
|
30 |
30 |
Thematic plan of office hours
OH theme |
Objectives |
Form of classes |
Contents of classes |
Recommended literature |
Subject 1 Introduction. Classification Internal and external coatings |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 2. Physical and chemical properties of solid surfaces |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 3. Physical and-chemical properties of the materials for the application of coatings |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 4. Thermal spray coating |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 5. Formation of thermal spray coatings |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 6. Vacuum condensation deposition coatings |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subject 7. Coating of molten of the states |
Increasing knowledge on this subject |
Report defense |
Lectures notes |
[1-4] |
Subjects of control tasks for AL
- Mechanical surface impact.
2. Thermal effect on surface.
3. Subjecting the surface to the thermal diffusion.
4. Subjecting the surface to high radiation and particle flows.
Criteria of students’ knowledge assessment
The examination mark is determined by course as the sum of the maximum indexes of progress on midterm controls (to 60%) and to final attestation (examination) (to 40%) and makes value to 100% according to the table.
Grade on alphabetic system |
Numerical equivalents |
Percentage |
Traditional system |
А А- |
4,0 3,67 |
95-100 90-94 |
Excellent |
В+ В В- |
3,33 3,0 2,67 |
85-89 80-84 75-79 |
Good |
С+ С С- D+ D- |
2,33 2,0 1,67 1,33 1,0 |
70-74 65-69 60-64 55-59 50-54 |
Satisfactory |
F |
0 |
0-49 |
Unsatisfactory |
Grade «A» (excellent) is put in the case if student during a term showed perfect knowledge of all program questions of course, and also of subjects of independent work, regularly handed over midterm tasks, showed independence in studying of theoretical and applied questions according to the main program of studied course, and also on extra program questions.
Grade «A-» (excellent) stipulates perfect knowledge of basic laws and processes, concepts, ability to generalization of theoretical questions of course, regular handing of midterm tasks of classroom and independent work.
Grade “B+” (good) is put in the case if student showed good and excellent knowledge of course questions, regularly handed over term tasks generally on “excellent” and some on “good”.
Grade “B” (good) is put in the case if student showed good knowledge of the questions opening the main maintenance of a concrete subject of course, and also subject of independent work, regularly handed over term tasks on “good” and “excellent”.
Grade “B-” (good) is put to a student in the case if he well is guided in theoretical and applied questions of course both on classroom, and on AL subjects, but irregularly handed over midterm tasks and had cases of a repeating an examination of term tasks on course.
Grade “C+” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “good” and “satisfactory” term tasks.
Grade “C” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “satisfactory” term tasks.
Grade “C-” (satisfactory) is put to a student in the case student during a term regularly handed over term tasks, but concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.
Grade “D+” (satisfactory) is put to a student in the case he irregularly handed over term tasks concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.
Grade “D-” (satisfactory) is put to a student in the case he irregularly handed over term tasks, concerning room classes and AL, owns the minimum volume of knowledge, and also allowed admissions of classes.
Grade “F” (unsatisfactorily) is put when student practically doesn’t own the minimum theoretical and practical material of room classes and AL on course, irregularly visits classes and doesn’t hand over in time term tasks.
Midterm control is carried out on the 7, 14 weeks of study and it develops proceeding from the following types of control:
Type of control |
Percentage |
Academic period of study, week |
in total, % |
||||||||||||||
1 |
2 |
3 |
4 |
5 |
6 |
7 |
8 |
9 |
10 |
11 |
12 |
13 |
14 |
15 |
|||
Attendance |
0,2 |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
* |
3 |
Lecture notes |
1 |
|
* |
|
* |
|
* |
|
* |
|
* |
|
* |
|
* |
|
7 |
Written test |
5 |
|
|
|
* |
|
|
|
|
* |
|
|
|
|
* |
|
15 |
AL |
6 |
|
|
* |
|
|
|
* |
|
|
|
* |
|
|
|
* |
24 |
Examintaion |
1 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
* |
1 |
Total on attestation |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
50 |
Total |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
100 |
Policies and procedures
At studying course «Protective coatings and refractory enamel» I ask to observe the following rules:
1. Do not be late for class.
2. Do not miss classes without good reason, in case of illness please provide help, in other cases – an explanatory note.
3. Actively participate in the learning process.
4. Be tolerant, open, frank and friendly to fellow students and teachers.
Educational-methodical provision of the course
Author |
Literature |
Publishing house, year of the issue |
Number of copies |
|
At library |
At department |
|||
Main literature |
||||
Bobrov G.V., A.A. Ilyin. | The application of inorganic coatings | 2004 |
7 |
|
M. Hocking, Vasantasri V., P. Sidky. | Metallic and ceramic coatings | 2000, |
10 |
|
Additional literature |
||||
Loganina V.I., L.P. Orentlikher. | Persistence of protective and decorative coatings exterior walls | 2000 |
10 |
|
Loganina V.I., L.P. Orentlikher. | The quality of finishing construction products and colorful compositions. | 2002 |
11 |
|
Schedule for the completion of tasks on course
Type of control |
The purpose and contents of the jod |
Recommended Reading |
Duration of |
Form of control |
Passing term |
Current |
Knowledge of the theoretical material |
[1-4] |
20 min |
Written test |
4,9,14 week |
Current |
Depth study of a given material |
[1-4] |
2 week |
Report |
during a term |
Midterm |
Knowledge of the technological features of the various methods of coating |
[1-4] |
30 min |
control work |
5,10,15 week |
final |
|
|
20 min |
examination |
May |
Questions for self-checking
1. What are the main indicators of quality of coatings ?
2 . How grounds are classified on?
3 . What methods are used to create the impact of internal coatings ?
4 . What does distinguish outer cover?
5 . What are the indicators of the effectiveness of the coating process ?
6. What is the cause of the surface layer ?
7. What is called a surface energy of what values is stack up?
8. What is called adsorption and how it affects the surface energy?
9. What is the difference between physical adsorption and chemisorption ?
10 . Which substances are considered to be physically adsorbed dirt surface of the material ?
11. How does saturation of the metallic coating by oxygen, nitrogen, hydrogen and carbon affect the coating properties?
12. In which case will oxidation reaction occur?
13. How does the oxygen affect metal ?
14. What condition may be present on the surface of the material moisture ?
15. What grounds are methods of thermal spraying classified on?
16. What are the parameters of spray ? How do they affect the heat efficiency spray ?
17. What does determines the effective efficiency heating ?
18. What are the parameters of the sprayed material ?
19. What parameters do characterize the external conditions of deposition ?
20. What is meant by the efficiency of the process ?
21 What value does take the loss of spray material into account?
22. What does determine the performance of the spraying process ?
23. What are the stages of interaction of particles with the surface of the deposition ?
24. What does determine the temperature in the contact area of particles ?
25. How high does the temperature in the spot spraying affect the quality indicators cover?
26. How does coating by vacuum condensation occur?
27. What grounds are methods of MNWC classified on?
28. What are the advantages and disadvantages of the method MNWC ?
29. What are the stages of the process is MNWC ?
30. What are parameters affect the efficiency of the process MNWC ?
31. How can molten material interact with the surface of the base material of the article ?
32. Which is considered to be a limiting process in the formation of a coating of molten material?
33. What are the surface tension acting on wetting solid -liquid?
34. What does determine value of the contact angle ?
35. What is the classification of the coatings from the molten state